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http://hdl.handle.net/20.500.12188/16143
Наслов: | In situ crystallization and crystal structure determination of chlorobenzene | Authors: | Nath, Naba K. Naumov, Panče |
Issue Date: | 19-мај-2015 | Publisher: | Society of Chemists and Technologists of Macedonia | Journal: | Macedonian Journal of Chemistry and Chemical Engineering | Abstract: | <jats:p><p>The crystal structure of chlorobenzene, which is liquid at ambient conditions of pressure and temperature, was determined after <em>in situ</em> crystallization by using Optical Heating and Crystallization Device (OHCD) coupled to a single crystal X-ray diffractometer. Chlorobenzene crystallizes in the orthorhombic space group <em>Pbcn</em> with one symmetry-independent molecule in the asymmetric unit. In the crystal structure, type II Cl Cl interactions form zigzag chains that are assisted by C—H π interactions. Hirshfeld surface analysis revealed five types of intermolecular contacts.</p></jats:p> | URI: | http://hdl.handle.net/20.500.12188/16143 | DOI: | 10.20450/mjcce.2015.682 |
Appears in Collections: | Faculty of Natural Sciences and Mathematics: Journal Articles |
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File | Опис | Size | Format | |
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XIII_2136.pdf | N. K. Nath, P. Naumov, In situ crystallization and crystal structure determination of chlorobenzene, Macedonian Journal of Chemistry and Chemical Engineering, 34(1) 63–66 (2015). | 674.39 kB | Adobe PDF | View/Open |
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